Instructor's Guide and Solutions Manual to Organic Structures From 2D NMR Spectra

Instructor's Guide and Solutions Manual to Organic Structures From 2D NMR Spectra

By: L. D. Field (author), A. M. Magill (author), H. L. Li (author)Paperback

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Description

The text Organic Structures from 2D NMR Spectra contains a graded set of structural problems employing 2D-NMR spectroscopy. The Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra is a set of step-by-step worked solutions to every problem in Organic Structures from 2D NMR Spectra. While it is absolutely clear that there are many ways to get to the correct solution of any of the problems, the instructors guide contains at least one complete pathway to every one of the questions. In addition, the instructors guide carefully rationalises every peak in every spectrum in relation to the correct structure. The Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra: Is a complete set of worked solutions to the problems contained in Organic Structures from 2D NMR Spectra. Provides a step-by-step description of the process to derive structures from spectra as well as annotated 2D spectra indicating the origin of every cross peak. Highlights common artefacts and re-enforces the important characteristics of the most common techniques 2D NMR techniques including COSY, NOESY, HMBC, TOCSY, CH-Correlation and multiplicity-edited C-H Correlation. This guide is an essential aid to those teachers, lecturers and instructors who use Organic Structures from 2D NMR as a text to teach students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry.

Contents

Preface ix Solutions Summary 1 Problem 1 (1-iodopropane) 7 Problem 2 (2-butanone) 11 Problem 3 (2-hexanone) 15 Problem 4 (ethyl propionate) 19 Problem 5 (ethyl 3-ethoxypropionate) 23 Problem 6 (4-acetylbutyric acid) 28 Problem 7 (3-ethoxypropionyl chloride) 32 Problem 8 (ethyl 3-chloropropionate) 36 Problem 9 (isoamyl acetate) 40 Problem 10 (trans-4-hexen-3-one) 45 Problem 11 (trans-2-octen-4-one) 50 Problem 12 (3-nitrobenzaldehyde) 55 Problem 13 (3-iodotoluene) 61 Problem 14 (8-hydroxy-5-nitroquinoline) 64 Problem 15 (2-bromo-3-picoline) 69 Problem 16 (trans-anethole) 72 Problem 17 (cis-2-pentene) 75 Problem 18 (p-tolyl benzoate) 79 Problem 19 (phenyl p-toluate) 86 Problem 20 (4-biphenylyl acetate) 93 Problem 21 (4'-phenoxyacetophenone) 99 Problem 22 (4'-tert-butylacetophenone) 106 Problem 23 (2,2,4'-trimethylpropiophenone) 110 Problem 24 (trans-2-methyl-3-phenyl-2-propen-1-ol) 114 Problem 25 (methyl 4-ethoxybenzoate) 119 Problem 26 (methyl 3-(p-tolyl)propionate) 123 Problem 27 (4-(4'-methoxyphenyl)-2-butanone) 127 Problem 28 (ethyl 6-bromohexanoate) 132 Problem 29 (piperonal) 135 Problem 30 (cis-3-hexenyl benzoate) 139 Problem 31 (trans-2,cis-6-nonadienal) 146 Problem 32 (allyl glycidyl ether) 155 Problem 33 (3,4-epoxy-4-methyl-2-pentanone) 159 Problem 34 (dl-methionine) 162 Problem 35 (N-acetyl-l-leucine) 165 Problem 36 (isoamyl valerate) 170 Problem 37 ((E)-4-methyl-4'-nitrostilbene) 173 Problem 38 (2-tert-butyl-6-methylphenol) 181 Problem 39 (2-allyl-6-methylphenol) 186 Problem 40 (2-hydroxy-4-methoxybenzaldehyde) 194 Problem 41 (2'-hydroxy-5'-methylacetophenone) 198 Problem 42 (3'-fluoro-4'-methoxyacetophenone) 203 Problem 43 (trans-ferulic acid) 209 Problem 44 (sec-butyl 3-hydroxycinnamate) 215 Problem 45 (1-benzosuberone) 221 Problem 46 (dimethyl (3-bromopropyl)phosphonate) 228 Problem 47 (caffeine) 233 Problem 48 (benzyloxypropionitrile) 238 Problem 49 (cineole) 242 Problem 50 (thymoquinone) 246 Problem 51 (4-bromo-1-indanol) 251 Problem 52 (1-bromo-4-methylnaphthalene) 257 Problem 53 (carvacrol) 264 Problem 54 (acetoacetanilide) 272 Problem 55 (ethyl acetamidocyanoacetate) 277 Problem 56 ( -humulene) 283 Problem 57 (3,4-dihydro-2H-benzopyran-3-carboxylic acid) 289 Problem 58 (quinidine) 296 Problem 59 (salbutamol) 312 Problem 60 (2-hydroxy-1-naphthaldehyde) 322 Problem 61 (6-methyl-4-chromanone) 329 Problem 62 (citronellal) 336 Problem 63 ((+)-cis-2-oxabicyclo-[3.3.0]oct-6-en-3-one) 344 Problem 64 (melatonin) 349 Problem 65 (carvone) 362 Problem 66 (haloperidol) 370

Product Details

  • ISBN13: 9781119027256
  • Format: Paperback
  • Number Of Pages: 392
  • ID: 9781119027256
  • weight: 1
  • ISBN10: 111902725X

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