Laboratory Techniques in Organic Chemistry (4th Revised edition)

Laboratory Techniques in Organic Chemistry (4th Revised edition)

By: Jerry R. Mohrig (author), Christina Noring Hammond (author), David Alberg (author), Gretchen Holifmeister (author), Paul F. Schatz (author)Paperback

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Description

Laboratory Techniques in Organic Chemistry is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. It is written to provide effective support for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments.

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About Author

Jerry Mohrig, Carleton College, USA. David Alberg, Carleton College, USA. Gretchen Holifmeister, Carleton College, USA. Paul F. Schatz, University of Wisconsin-Madison, USA. Christina Noring Hammond, Vassar College, USA.

Contents

PART I: INTRODUCTION TO THE ORGANIC LABORATORY Essay: Introduction to the Organic Laboratory 1. Safety in the Laboratory 2. Protecting the Environment 3. Laboratory Notebooks and Prelaboratory Information PART II: CARRYING OUT CHEMICAL REACTIONS Essay: Carrying Out Chemical Reactions 4. Laboratory Glassware 5. Measurements and Transferring Reagents 6. Heating and Cooling Methods 7. Carrying out Organic Reactions 8. Computational Chemistry PART III: BASIC METHODS FOR SEPARATION, PURIFICATION, AND ANALYSIS Essay: Intermolecular Forces in Organic Chemistry 9. Filtration 10. Extraction 11. Drying Organic Liquids and Recovering Reaction Products 12. Boiling Points and Distillation 13. Refractometry 14. Melting Points and Melting Ranges 15. Recrystallization 16. Sublimation 17. Optical Activity and Enantiomeric Analysis PART IV: CHROMATOGRAPHY Essay: Modern Chromatographic Separations 18. Thin-Layer Chromatography 19. Liquid Chromatography 20. Gas Chromatography PART V: SPECTROMETRIC CHARACTERIZATION METHODS Essay: The Spectrometric Revolution 21. Infrared Spectroscopy 22. Nuclear Magnetic Resonance Spectroscopy 23. 13C and Two-Dimensional NMR Spectroscopy 24. Mass Spectrometry 25. Ultraviolet and Visible Spectroscopy 26 . Integrated Spectrometry Problems PART VI: DESIGNING AND CARRYING OUT ORGANIC EXPERIMENTS 27. Using the Literature of Organic Chemistry 28. Designing a Chemical Reaction

Product Details

  • publication date: 13/05/2014
  • ISBN13: 9781464134227
  • Format: Paperback
  • Number Of Pages: 528
  • ID: 9781464134227
  • weight: 727
  • ISBN10: 1464134227
  • edition: 4th Revised edition

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