Microwaves in Nanoparticle Synthesis: Fundamentals and Applications

Microwaves in Nanoparticle Synthesis: Fundamentals and Applications

By: Nick Serpone (editor), Satoshi Horikoshi (editor)Hardback

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Description

For the first time, this comprehensive handbook presents the emerging field of microwave technology for the synthesis of nanoparticles. Divided into three parts--fundamentals, methods, and applications--it covers topics including microwave theory, scale-up, microwave plasma synthesis, characterization, and more. This offers both an important volume for academic researchers, and a resource for those in industry exploring the applications of nanoparticles in semiconductors, electronics, catalysis, sensors, and more.

About Author

Satoshi Horikoshi received his PhD degree in 1999 from Meisei University, and subsequently was a postdoctoral researcher at the Frontier Research Center for the Global Environment Science unitl 2006. He joined Sophia University as Assistant Professor in 2006, and then moved to Tokyo University of Science as an associate professor in 2008. He is currently the Vice-President of the Japan Society of Electromagnetic Wave Energy Applications, a Member of the Board of the International Microwave Power Institute, and the Editorial Advisory Board of Mini-Reviews in Organic Chemistry.His research interests include the application of microwave radiation to catalytic chemistry, to the effects of microwaves on photocatalysts for environmental protection, to the microwave-assisted organic syntheses, and to microwave effects on nanoparticles. He has authored over 110 scientific publications. Nick Serpone received his Ph.D. from Cornell University (Physical-Inorganic Chemistry, 1968), after which he joined Concordia University in Montreal as Assistant Professor (1968-73), Associate Professor (1973-1980), and Professor (1980-1998). He was a consultant to 3M?s Imaging Sector for over 10 years. He took early retirement from Concordia University (1998) and was made a University Research Professor (1998-2004) and Professor Emeritus (2000 to present). He was Program Director at NSF (1998-2001) and has been a Visiting Professor at the University of Pavia, Italy, since 2002. His research interests are currently in the photophysics and photochemistry of semiconductor metal oxides, heterogeneous photocatalysis, environmental photochemistry, photochemistry of sunscreen active agents, and application of microwaves to nanomaterials and to environmental remediation. He has co-authored over 400 articles and has co-edited four monographs (for Wiley, Elsevier and the American Chemical Society).

Contents

PREFACE INTRODUCTION TO NANOPARTICLES General Introduction to Nanoparticles Methods of Nanoparticle Synthesis Surface Plasmon Resonance and Coloring Control of Size, Shape, and Structure Reducing Agent in Nanoparticle Synthesis Applications of Metallic Nanoparticles GENERAL FEATURES OF MICROWAVE CHEMISTRY Microwave Heating Some Applications of Microwave Heating Microwave Chemistry Microwave Chemical Reaction Equipment CONSIDERATIONS OF MICROWAVE HEATING General Considerations of Microwave Heating Peculiar Microwave Heating Relevant Points of Effective Microwave Heating COMBINED ENERGY SOURCES IN THE SYNTHESIS OF NANOMATERIALS Introduction Simultaneous Ultrasound/Microwave Treatments Sequential Ultrasound and Microwaves Conclusions NANOPARTICLE SYNTHESIS THROUGH MICROWAVE HEATING Introduction Microwave Frequency Effects Nanoparticle Synthesis under a Microwave Magnetic Field Synthesis of Metal Nanoparticles by a Greener Microwave Hydrothermal Method Nanoparticle Synthesis with Microwaves under Cooling Conditions Positive Aspects of Microwaves - Thermal Distribution in Nanoparticle Synthesis Microwave-Assisted Nanoparticle Synthesis in Continuous Flow Apparatuses MICROWAVE-ASSISTED SOLUTION SYNTHESIS OF NANOMATERIALS Introduction Synthesis of ZnO Nanocrystals Synthesis of a-Fe2O3 Nanostructures Element-Based Nanostructures and Nanocomposite Chalcogenide Nanostructures Graphene Summary PRECISELY CONTROLLED SYNTHESIS OF METAL NANOPARTICLES UNDER MICROWAVE IRRADIATION Introduction Precise Control of Single Component under Microwave Irradiation Precise Control of Multicomponent Structures under Microwave Irradiation An Example of Mass Production Oriented to Application Conclusion MICROWAVE-ASSISTED NONAQUEOUS ROUTES TO METAL OXIDE NANOPARTICLES AND NANOSTRUCTURES Introduction Nonaqueous Sol - Gel Chemistry Polyol Route Benzyl Alcohol Route Other Mono-Alcohols Ionic Liquids Nonaqueous Microwave Chemistry beyond Metal Oxides Summary and Outlook INPUT OF MICROWAVES FOR NANOCRYSTAL SYNTHESIS AND SURFACE FUNCTIONALIZATION FOCUS ON IRON OXIDE NANOPARTICLES Introduction Biomedical Applications of Iron Oxide Nanoparticles Nanoparticle Synthesis Nanoparticle Surface Functionalization Microwave-Assisted Chemistry Conclusions MICROWAVE-ASSISTED CONTINUOUS SYNTHESIS OF INORGANIC NANOMATERIALS Introduction and Overview Microwave-Assisted Continuous Synthesis of Inorganic Nanomaterials Types of Microwave Apparatus Used in Continuous Synthesis Microwave Continuous Synthesis of Molecular Sieve Materials Microwave Continuous Synthesis of Metal Oxides and Mixed Metal Oxide Materials Microwave Continuous Synthesis of Metallic Nanomaterials Conclusions and Outlook MICROWAVE PLASMA SYNTHESIS OF NANOPARTICLES: FROM THEORETICAL BACKGROUND AND EXPERIMENTAL REALIZATION TO NANOPARTICLES WITH SPECIAL PROPERTIES Introduction Using Microwave Plasmas for Nanoparticle Synthesis Experimental Realization of the Microwave Plasma Synthesis Infl uence of Experimental Parameters Nanoparticle Properties and Application Summary OXIDATION, PURIFI CATION AND FUNCTIONALIZATION OF CARBON NANOTUBES UNDER MICROWAVE IRRADIATION Introduction Oxidation and Purifi cation Functionalization Conclusion INDEX

Product Details

  • ISBN13: 9783527331970
  • Format: Hardback
  • Number Of Pages: 352
  • ID: 9783527331970
  • weight: 902
  • ISBN10: 3527331972

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